{"id":1601,"date":"2018-08-08T16:09:07","date_gmt":"2018-08-08T23:09:07","guid":{"rendered":"http:\/\/rccostello.com\/wordpress\/?p=1601"},"modified":"2026-05-08T04:06:47","modified_gmt":"2026-05-08T11:06:47","slug":"spinning-tube-reactor-flow-chemistry","status":"publish","type":"post","link":"https:\/\/www.rccostello.com\/wordpress\/modular-plants\/spinning-tube-reactor-flow-chemistry\/","title":{"rendered":"Utilizing the Spinning Tube in a Tube\u00ae Reactor in Flow Chemistry"},"content":{"rendered":"<p>On&nbsp;July 31, 2018 our CEO, Mr. Rocky Costello, P.E., gave a presentation titled &#8220;Utilizing the Spinning Tube in a Tube<sup>\u00ae<\/sup> Reactor in Flow Chemistry&#8221; at the Annual Congress on Medicinal Chemistry, Pharmacology and Toxicology conference in Amsterdam. The&nbsp;subjects that Mr. Costello discussed include the following four topics:<\/p>\n<ol>\n<li>STT<sup>\u00ae<\/sup> Discovery<\/li>\n<li>Patented Technology<\/li>\n<li>Research<\/li>\n<li>Application<\/li>\n<\/ol>\n<p>A detailed explanation of the calculation of Reynolds number in piping systems and then rotating systems were also discussed.<\/p>\n<p>The&nbsp;chart&nbsp;below shows various rotating flow regimes such as Couette flow and Taylor- Vortex flow inside the Spinning Tube in a Tube Reactor<sup>\u00ae<\/sup>, or STT<sup>\u00ae<\/sup>. It is essentially a graph of Reynolds number calculated with respect to the outer cylinder versus <span style=\"display: inline !important; float: none; background-color: transparent; color: #333333; cursor: text; font-family: Georgia,'Times New Roman','Bitstream Charter',Times,serif; font-size: 16px; font-style: normal; font-variant: normal; font-weight: 400; letter-spacing: normal; orphans: 2; text-align: left; text-decoration: none; text-indent: 0px; text-transform: none; -webkit-text-stroke-width: 0px; white-space: normal; word-spacing: 0px;\">Reynolds number calculated with respect to the inner cylinder.&nbsp; <\/span>The flow regimes for two (2) independently rotating cylinders is shown. Since the outer cylinder is not rotating the Reynolds number on the&nbsp;&#8220;X&#8221; axis is zero.&nbsp; The area of concern is the flow regimes inside the red box.<\/p>\n<p><a href=\"http:\/\/rccostello.com\/wordpress\/wp-content\/uploads\/2018\/08\/Flow-Regimes.png\"><img loading=\"lazy\" decoding=\"async\" class=\"aligncenter wp-image-1630 size-full\" title=\"Flow Regimes in a Spinning Tube in a Tube\" src=\"http:\/\/rccostello.com\/wordpress\/wp-content\/uploads\/2018\/08\/Flow-Regimes.png\" alt=\"Spinning Tube in a Tube\u00ae\" width=\"737\" height=\"528\" srcset=\"https:\/\/www.rccostello.com\/wordpress\/wp-content\/uploads\/2018\/08\/Flow-Regimes.png 737w, https:\/\/www.rccostello.com\/wordpress\/wp-content\/uploads\/2018\/08\/Flow-Regimes-300x215.png 300w\" sizes=\"auto, (max-width: 737px) 100vw, 737px\" \/><\/a><\/p>\n<p>In a YouTube video, the STT<sup>\u00ae<\/sup> with a glass stator demonstrates the transition from high Reynold number, turbulent flow and Taylor Rings to low <span style=\"display: inline !important; float: none; background-color: transparent; color: #333333; cursor: text; font-family: Georgia,'Times New Roman','Bitstream Charter',Times,serif; font-size: 16px; font-style: normal; font-variant: normal; font-weight: 400; letter-spacing: normal; orphans: 2; text-align: left; text-decoration: none; text-indent: 0px; text-transform: none; -webkit-text-stroke-width: 0px; white-space: normal; word-spacing: 0px;\">Reynold number, laminar flow and Couette flow.&nbsp; It also demonstrates how simplified Clean-In-Place is accomplished with the&nbsp;STT<sup>\u00ae<\/sup>.<\/span><\/p>\n<p><iframe loading=\"lazy\" title=\"STT Visual Demo\" width=\"500\" height=\"375\" src=\"https:\/\/www.youtube.com\/embed\/djj3RjRpuCc?feature=oembed\" frameborder=\"0\" allow=\"accelerometer; autoplay; clipboard-write; encrypted-media; gyroscope; picture-in-picture; web-share\" referrerpolicy=\"strict-origin-when-cross-origin\" allowfullscreen><\/iframe><\/p>\n<h3>Spinning Tube in a Tube<sup>\u00ae<!--?sup &gt;&lt;span data-mce-type=\"bookmark\" style=\"display: inline-block; width: 0px; overflow: hidden; line-height: 0;\" class=\"mce_SELRES_start\"&gt;&lt;\/span&gt; technology has broad commercial applications.&lt;\/h3&gt; &lt;ul&gt; &lt;li&gt;Chemical Synthesis&lt;\/li&gt; &lt;li&gt;Polymer Synthesis and Modification (narrow chain length distribution since hot vessel walls create longer polymers)&lt;\/li&gt; &lt;li&gt;Solids Synthesis&lt;\/li&gt; &lt;li&gt;Mixing - Dispersing\/Blending\/Compounding\/ Emulsification\/Suspensions&lt;\/li&gt; &lt;li&gt;Biocatalysts and Bioprocessing&lt;\/li&gt; &lt;li&gt;Extractions\/Separations&lt;\/li&gt; &lt;li&gt;Nanoparticle Synthesis and Catalysis&lt;\/li&gt; &lt;\/ul&gt; &lt;p&gt;A potential flow sheet for the STT\u00a0utilizing nanoparticle catalysis is shown below.&lt;\/p&gt; &lt;p&gt;&lt;a href=\"http:\/\/rccostello.com\/wordpress\/wp-content\/uploads\/2018\/08\/nanoparticle-catalysis.png\"&gt;&lt;img class=\"aligncenter wp-image-1641 size-full\" title=\"STT with Nanoparticle Catalysis\" src=\"http:\/\/rccostello.com\/wordpress\/wp-content\/uploads\/2018\/08\/nanoparticle-catalysis.png\" alt=\"Spinning Tube in a Tube\u00ae\" width=\"758\" height=\"473\" ?--><\/sup><\/h3>\n<p>Comsol Computational Fluid Dynamics was used to model experimental runs of the Ritter reaction performed on the STT<sup>\u00ae<\/sup>&nbsp;at the EPA.<\/p>\n<p>Tertiary butyl alcohol reacted with&nbsp;benzonitrile to create N-tert-butylbenzamide.<\/p>\n<p>So why model the Spinning Tube in a Tube<sup>\u00ae<\/sup>&nbsp;System?<\/p>\n<ul>\n<li>Enhanced experimental design<\/li>\n<li>Reduced R&amp;D costs for product development<\/li>\n<li>Knowledge to explain STT&nbsp;performance to potential industrial users<\/li>\n<\/ul>\n<p>The full presentation can be downloaded here:&nbsp;<a href=\"http:\/\/rccostello.com\/Amsterdam%20Presentation%20Final%2031%20July%202018.pdf\">Utilizing the Spinning Tube in a Tube<sup>\u00ae<\/sup> Reactor in Flow Chemistry<\/a><\/p>\n<p>The STT<sup>\u00ae <\/sup>Technology is owned by <a href=\"http:\/\/brightpathlabs.com\/\">Bright Path Laboratories<\/a>.<\/p>\n<p>References:<br \/>\n1. Flow regimes in a circular Couette system with independently rotating cylinders By C. DAVID ANDERECKT, S. S. LIUS AND HARRY L. SWINNEY Department of Physics, The University of Texas, Austin, Texas 78712 (Received 20th December 1984 and in revised form 8th September 1985)<br \/>\n2. Kinetics of Transesterification of Soybean Oil, H. Noureddini and D. Zhu, Department of Chemical<br \/>\nEngineering, University of Nebraska, JAOCS, Vol 74, no. 11 (1997)<br \/>\n3. S. Cerbelli et al. \/ Chemical Engineering Science 63 (2008) 4396-4411<\/p>\n<h1 style=\"text-align: center;\"><a href=\"http:\/\/rccostello.com\/\">COSTELLO<\/a><\/h1>\n<h1 style=\"text-align: center;\">implements one-of-a-kind process engineering with exceptional knowledge and experience, process safety support and superior customer service.<\/h1>\n<h2 style=\"text-align: center;\">Contact us today for your Flow Chemistry Projects!<\/h2>\n","protected":false},"excerpt":{"rendered":"<p>On&nbsp;July 31, 2018 our CEO, Mr. Rocky Costello, P.E., gave a presentation titled &#8220;Utilizing the Spinning Tube in a Tube\u00ae Reactor in Flow Chemistry&#8221; at the Annual Congress on Medicinal Chemistry, Pharmacology and Toxicology conference in Amsterdam. The&nbsp;subjects that Mr. Costello discussed include the following four topics: STT\u00ae Discovery Patented Technology Research Application A detailed [&hellip;]<\/p>\n","protected":false},"author":15,"featured_media":1630,"comment_status":"closed","ping_status":"open","sticky":false,"template":"","format":"standard","meta":{"_genesis_hide_title":false,"_genesis_hide_breadcrumbs":false,"_genesis_hide_singular_image":false,"_genesis_hide_footer_widgets":false,"_genesis_custom_body_class":"","_genesis_custom_post_class":"","_genesis_layout":"","footnotes":""},"categories":[1],"tags":[114,109,14,74,174,187,93,73,188],"class_list":["post-1601","post","type-post","status-publish","format-standard","has-post-thumbnail","category-modular-plants","tag-chemical-engineering","tag-costello","tag-engineering-solutions","tag-environment","tag-flow-chemistry","tag-process-flow","tag-process-intensification","tag-safety","tag-spinning-tube-in-a-tube","entry"],"yoast_head":"<!-- This site is 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